Equipment List

New breakthroughs

Drawing on our expertise and research, we serve the diverse needs of the community, Nebraska and beyond. Our faculty is dedicated to enabling students to use scientific approaches to discovery and understanding.
New breakthroughs

Drawing on our expertise and research, we serve the diverse needs of the community, Nebraska and beyond. Our faculty is dedicated to enabling students to use scientific approaches to discovery and understanding.

Equipment List

The Dept. of Chemistry at UNK houses a wide range of basic and advanced research instrumentations available for both faculty and student use. You can view all of the equipment in the image gallery below.

Entries marked with asterisk (*) indicate equipments purchased with external grants or private funds.

Jasco J-810 Circular Dichroism Spectropolarimeter (2013)

Cary UV-Vis spectrophotometer (2014)

Delong America, Inc. LVEM-5 (Low-voltage Electron Microscope) with TEM, SEM, STEM and ED imaging modes (2011)*

Nuclear Magnetic Resonance Spectrometer Bruker Avance 300 MHz with variable temperature controller, multiple probes, Z-gradient, and network capabilities (2001) *

Isothermal Titration Calorimetry (2013) - TA instruments nanoITC

Agilent 7820A GC-MS (5975 series MSD) with autosampler (2011)

Powder X-Ray diffraction spectrometer

TA Instruments Simultaneous Differential Thermal Analyzer (TGA/DSC) Q600 (2011)

TA Instruments Differential Scanning Calorimeter Q20 (2011)

Veeco Dektak 150 Stylus Profiler (2010)*

Custom-built DC Thin Film Sputtering System (2010)*

Varian 720-ES Axial ICP Optical Emission Spectrometer (2009)*

Bioanalytical Systems PWR-3 Power Module/Potentiostat (2008)

Gaussian '09 Work station (2013)

Horiba/Jobin Yvon LabRAM HR800 Raman Microscope (2007)*

Horiba/Jobin Yvon FluoroMax-4 steady-state fluorometer (2010)

Thermo Nicolet IR200 FTIR Spectrometer System (2007): 7800 to 375 cm^-1 spectral range and 16 to 4 cm^-1 resolution; used in organic teaching lab

Biotek Synergy 2 UV/Vis/Fluorescent Microplate Reader with Dispenser System (2006)

Custom-built Physical Vapor Deposition apparatus with 8000W Quad Ellipse Chamber Heat and Model 915 Power Supply/Temperature Controller from Research Inc. Includes turbo-molecular and roughing pumps (2006) GE AKTA Prime Fast Protein Liquid Chromatography System (2005) Hewlett-Packard Agilent 8453 UV-vis Spectrophotometer with 200-1100 nm scanning range (2004)*

Eppendorf PCR Thermocycler (2004) Waters Gradient High-Performance Liquid Chromatograph System (2003)

UNIlab mBraun glovebox (2011)*

FTIR spectrometer: Thermo Nicolet Nexus 670 System with near- and far-IR scanning and detection capabilities. 0.09 cm^-1 resolution and scanning speeds up to 65 scans per second (2003)

Thermoquest Trace 2000 Series GC with Finnegan Polaris MS (1999)*

Nitrogen dye laser, argon laser, and CCD detector used for Fluorescence, Raman, and Excited-State Lifetime measurement capabilities (1999)*

Johnson-Matthey Mark I Magnetic Susceptibility Balance (1998)

Silicon Graphics Octane Workstation with Spartan molecular modeling software, color printer, CD-ROM, DAT drive, and World Wide Web server software (1997)*

Autoclave: Tuttnauer Model 3870E (1996)*

Incubators: Innova Model 4000 (1996)*; Fischer Precision (1996)*

Electrophoresis equipment: 2 Bio-Rad Model 1000/500 power supplies, 6 Protean III, Protean II, 2 Model 583 Gel driers, 2 Sub-cell cells with gel tray, 3 Sequigen II/powerpac 3000 system, Gel doc 1000 UV documentation system (1996, 2002)

Refrigerated Centrifuge: Beckman Avanti J25 (1995)*

Desktop-size low-voltage electron microscope with SEM, TEM, STEM, and ED modes.

This Nuclear Magnetic Resonance Spectrometer was purchased in 2001 with a grant from the University of Nebraska Foundation. It includes a broadband probe, variable temperature controller, Z-gradient 2-D acquisition, and network capabilities.

TA instrument NANO ITC

Agilent 7820 A GC-MS with autosampler. This instrument includes an autosampler and enhances molecular structure characterization capabilities in our organic and analytical chemistry areas.

$This Spectrum One liquid-nitrogen cooled CCD array spectrograph is outfitted with both 600 groove/mm and 2400 groove/mm gratings. In normal resolution mode (for fluorescence measurements) the instrument has a resolution of 0.15 nm throughout the ultraviolet-visible spectrum. It is capable of achieving signal to noise ratios in excess of 10,000 in a fraction of a second while simultaneously measuring all wavelengths in a 150-nm window. In high resolution mode (for Raman spectroscopy), the instrument has a resolution of 0.035 nm (about 1.5 cm-1 near 488 nm). Excellent quality spectra can be taken in about one minute for pure samples or a few minutes for proteins in solution.$

This Spectrum One liquid-nitrogen cooled CCD array spectrograph is outfitted with both 600 groove/mm and 2400 groove/mm gratings. In normal resolution mode (for fluorescence measurements) the instrument has a resolution of 0.15 nm throughout the ultraviolet-visible spectrum. It is capable of achieving signal to noise ratios in excess of 10,000 in a fraction of a second while simultaneously measuring all wavelengths in a 150-nm window. In high resolution mode (for Raman spectroscopy), the instrument has a resolution of 0.035 nm (about 1.5 cm-1 near 488 nm). Excellent quality spectra can be taken in about one minute for pure samples or a few minutes for proteins in solution.

Jasco J-810 circular dichroism spectropolarimeter

Custom-built vapor deposition apparatus. This custom-built apparatus is used to selenize and anneal (heat) solid-state materials samples. The 8000W Quad Ellipse Chamber Heater shown has manual and computer temperature control options with a maximum heating temperature of approx. 1000 oC. The tubular quartz sample chamber may be evaculated or flushed with a gas of choice.

The differential scanning calorimeter measures heat transfer during material phase changes.

Horiba Jobin Yvon FluoroMax-4 steady-state fluorescence spectrometer

FT-IR spectrometer. This instrument scans in the near-, mid-, and far-infrared regions with resolution down to 0.09 cm -1 and scanning speeds up to 65 scans per second. Detectors employed are a liquid nitrogen-cooled MCT (mercury-cadmium-telluride) detector for the near- and mid-IR regions and a polyethylene film detector for the far-IR region. Included are three beamsplitters: quartz (near), KBr (mid), and solid substrate (far). The department also has the following sampling accessories: traditional disk and solution cell holders, diffuse reflectance, specular reflectance (fixed 30 deg and a VeeMax II accessory for variable 30-80 degree incidence), and horizontal attenuated total reflectance (HATR). Classes and research groups utilize this instrument for characterization of organic and inorganic chemical reaction products as well as thin solar cell material films. Instrument features include spectral substraction, mathematical correction, baseline correction, and a library of thousands of reference IR spectra.

Gaussian '09 workstation

Varian 720 ICP OES. This Inductively Coupled Plasma-Optical Emission Spectrometer is used for metal trace-level and stoichiometric analysis of inorganic compound and material samples.

Inova 4000. This instrument is used by students in our biochemistry teaching and research laboratories.

LAB-RAM Hr800. This instrument is used to acquire Raman spectra of solid-state samples. Vibrational frequencies as low as 75 cm-1 may be observed. Includes CCD detector and optical imaging that enables focus on individual particles as small as 10 micrometers in diameter.

Biotek Synergy 2 UV/vis/Fluorescence Microplate Reader with Dispenser System

Nitrogen die, argon laser. Fuorescence (broadband and laser-induced) and Raman spectroscopy can be performed using this system, which was purchased through a grant from the University of Nebraska Foundation.

Eppendorf PCR Thermocycler

TA instruments Q600 simultaneous differential thermogravimetric analyzer. Simultaneous thermgravimetric analysis (TGA) and differential scanning calorimetry (DSC) can be performed on this instrument.

Custom built thin film sputtering system. This DC thin-film sputtering chanber is used for the fabrication of metal and metal oxide thin films in solar cell materials research.

UV Visible

Veeco dektak 150. For measurement of thin film thicknesses and roughness that range from 10 nm to several hundred microns.

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